{"id":6735,"date":"2023-05-17T17:20:15","date_gmt":"2023-05-17T09:20:15","guid":{"rendered":"\/\/www.progesta-pro.com\/?p=6735"},"modified":"2023-05-17T17:20:15","modified_gmt":"2023-05-17T09:20:15","slug":"acs-catal-%e9%9d%a2%e5%90%91%e9%80%83%e9%80%b8%e6%b0%a8%e7%9a%84%e6%8e%92%e6%94%be%e6%8e%a7%e5%88%b6cuox-ptcu%e5%82%ac%e5%8c%96%e5%89%82-%e7%aa%81%e7%a0%b4%e5%bc%82%e7%9b%b8","status":"publish","type":"post","link":"\/\/www.progesta-pro.com\/archives\/6735","title":{"rendered":"ACS Catal. | \u9762\u5411\u9003\u9038\u6c28\u7684\u6392\u653e\u63a7\u5236CuOx\/PtCu\u50ac\u5316\u5242\u2014\u2014\u7a81\u7834\u5f02\u76f8\u50ac\u5316\u6d3b\u6027\u548c\u9009\u62e9\u6027\u96be\u4ee5\u517c\u987e\u7684\u74f6\u9888<\/strong>"},"content":{"rendered":"\n

\u6c28\u6c14\u662fPM2.5\u7684\u91cd\u8981\u6765\u6e90\u4e4b\u4e00\uff0c\u5bf9\u4eba\u4f53\u5065\u5eb7\u548c\u5927\u6c14\u73af\u5883\u5177\u6709\u4e25\u91cd\u5371\u5bb3\u3002\u5927\u6c14\u4e2d\u6c28\u6c14\u7684\u6765\u6e90\u5305\u62ec\u81ea\u7136\u6e90\u548c\u4eba\u4e3a\u6e90\uff0c\u79fb\u52a8\u6e90\u67f4\u6cb9\u8f66\u5c3e\u6c14\u5904\u7406\u8fc7\u7a0b\u4e2d\uff0c\u5c3f\u7d20\u55b7\u6dcb\u4f1a\u9020\u6210\u672b\u7aef\u6c28\u6c14\u7684\u6cc4\u6f0f\u3002\u8fd1\u5e74\u6765\uff0c\u56fd\u52a1\u9662\u5bf9\u4e8e\u67f4\u6cb9\u8f66\u6392\u653e\u8981\u6c42\u8d8a\u53d1\u4e25\u82db\uff0c\u6211\u56fd\u4e8e21\u5e74\u6b63\u5f0f\u5b9e\u65bd\u7684\u91cd\u578b\u67f4\u6cb9\u8f66\u56fd\u516da\u6807\u51c6\uff0c\u89c4\u5b9a\u6c28\u6c14\u7684\u6392\u653e\u9650\u503c\u4ec5\u4e3a10ppm\uff0c\u8fdc\u4f4e\u4e8e\u6b27\u4e03\u6807\u51c6\u6392\u653e\u9650\u503c20 ppm\u3002\u4e4b\u524d\u901a\u7528\u7684\u91cd\u578b\u67f4\u6cb9\u8f66\u540e\u5904\u7406\u7cfb\u7edf\u4e3b\u8981\u7531\u67f4\u6cb9\u6c27\u5316\u50ac\u5316\u5668\uff08DOC\uff09\u3001\u67f4\u6cb9\u9897\u7c92\u6355\u96c6\u5668\uff08DPF\uff09\u548c\u9009\u62e9\u6027\u50ac\u5316\u8fd8\u539f\u53cd\u5e94\u5668\uff08SCR\uff09\u7ec4\u6210\uff0c\u800cSCR\u53cd\u5e94\u5668\u4e2d\u5c3f\u7d20\u7684\u8fc7\u91cf\u55b7\u6dcb\u5f88\u53ef\u80fd\u6392\u51fa\u8fc7\u91cf\u7684\u9003\u9038\u6c28\u3002\u8003\u8651\u5230\u6cc4\u6f0f\u6c28\u6c14\u7684\u5371\u5bb3\u548c\u65e5\u76ca\u4e25\u82db\u7684\u6392\u653e\u6cd5\u89c4\uff0c\u6545\u4e9f\u9700\u5728SCR\u672b\u7aef\u5b89\u88c5\u6c28\u9003\u9038\u50ac\u5316\u5668\uff08ASC\uff09\uff0c\u8fdb\u4e00\u6b65\u964d\u4f4e\u5c3e\u6c14\u4e2d\u7684\u6c28\u6c14\u542b\u91cf\uff0c\u5982\u56fe1<\/strong>\u6240\u793a\u3002<\/p>\n\n\n

\n
\"\"<\/a>
\u56fe1\uff1a<\/strong>\u91cd\u578b\u67f4\u6cb9\u8f66\u540e\u5904\u7406\u7cfb\u7edf\u67b6\u6784\u56fe<\/figcaption><\/figure><\/div>\n\n\n

ASC\u50ac\u5316\u5242\u53ef\u5c06NH3<\/sub>\u6c27\u5316\u4e3aN2<\/sub>\uff0c\u6210\u4e3a\u8d85\u4f4e\u6392\u653e\u67f4\u6cb9\u8f66\u7684\u5fc5\u5907\u540e\u5904\u7406\u50ac\u5316\u6280\u672f\u3002\u76f8\u6bd4\u4e8e\u73b0\u6709\u7684\u8d35\u91d1\u5c5e\uff08Pd, Au\uff09\u548c\u975e\u8d35\u91d1\u5c5e\u50ac\u5316\u6750\u6599\uff08CuOx\u7b49\uff09\uff0c\u8d1f\u8f7d\u578bPt\u57fa\u50ac\u5316\u5242\u662f\u76ee\u524d\u62a5\u5bfc\u7684\u50ac\u5316\u6d3b\u6027\u6700\u4f73\u7684\u9003\u9038\u6c28\u6d88\u9664ASC\u50ac\u5316\u5242\uff0c\u7531\u4e8ePt\u672c\u5f81\u6c27\u5316\u6d3b\u6027\u5f3a\uff0c\u751f\u6210\u526f\u4ea7\u7269NOx<\/sub>\u8f83\u591a\u7684\u74f6\u9888\u96be\u4ee5\u7a81\u7834\u3002Pt\u57fa\u50ac\u5316\u5242\u8868\u9762\u7684NH3<\/sub>\u6c27\u5316\u53cd\u5e94\u5e38\u5e38\u5171\u5b58\u7740\u9170\u4e9a\u80fa\u548c\u8054\u80fa\u673a\u7406\uff0c\u4e24\u79cd\u673a\u7406\u5177\u6709\u4ee5\u4e0b\u7279\u70b9\uff1a\u9170\u4e9a\u80fa\u673a\u7406\u6d3b\u6027\u9ad8\u3001N2<\/s>\u9009\u62e9\u6027\u4f4e\uff1b\u8054\u80fa\u673a\u7406\u6d3b\u6027\u4f4e\u3001N2<\/sub>\u9009\u62e9\u6027\u9ad8\u3002\u7531\u4e8e\u4e24\u8005NH3<\/sub>\u5feb\u901f\u6c27\u5316\u8131\u6c22\u548cN\u7269\u79cd\u8fc7\u5ea6\u6c27\u5316\u4f9d\u8d56\u540c\u4e00\u6c27\u7269\u79cd\uff08\u6d3b\u6027\u6c27O*\uff09\uff0c\u5176NH3<\/sub>\u9009\u62e9\u6027\u6c27\u5316\u7684\u50ac\u5316\u6d3b\u6027\u4e0e\u9009\u62e9\u6027\u5448\u73b0\u51fa\u8d1f\u76f8\u5173\uff0c\u5bfc\u81f4\u4e86\u76ee\u524dPt\u57fa\u50ac\u5316\u5242\u7684\u9ad8\u4f4e\u6e29\u6d3b\u6027\u4e0e\u9ad8N2<\/sub>\u9009\u62e9\u6027\u96be\u4ee5\u517c\u987e\u3002<\/p>\n\n\n\n

\u9488\u5bf9\u4e0a\u8ff0\u5173\u952e\u95ee\u9898\uff0c\u534e\u4e2d\u79d1\u6280\u5927\u5b66\u6750\u6599\u5b66\u9662\u5355\u658c\u6559\u6388\u56e2\u961f\u8bbe\u8ba1\u4e86\u4e00\u79cdPt-Cu\u03b4+<\/sup>\u53cc\u4f4d\u70b9\u50ac\u5316\u5242\uff0c\u8be5\u50ac\u5316\u5242\u8868\u73b0\u51fa\u4e8695%\u7684N2<\/sub>\u9009\u62e9\u6027\uff0c\u4e14\u8f6c\u5316\u9891\u7387\uff08TOFs\uff09\u503c\u8fdc\u9ad8\u4e8e\u76ee\u524d\u62a5\u9053\u7684\u5176\u4ed6Pt\u57fa\u50ac\u5316\u5242\u3002\u540c\u65f6\uff0c\u8be5\u5de5\u4f5c\u9996\u6b21\u53d1\u73b0\u4e86\u6676\u683c\u6c27\u8f85\u52a9\u7684i-SCR\u673a\u5236\uff0c\u5e76\u4e14\u6df1\u5ea6\u9610\u8ff0\u4e86\u5173\u952e\u4e2d\u95f4\u4ea7\u7269\u7684\u5f62\u6210\u8fc7\u7a0b\u548c\u5206\u89e3\u8fc7\u7a0b\u3002\u76f8\u5173\u6210\u679c\u4ee5\u201cUnraveling Lattice O Assisted i-SCR Mechanism on High N2<\/sub>\u00a0Selectivity of CuOx<\/sub>\/PtCu Catalysts in NH3<\/sub>-SCO\u201d\uff08\u9610\u8ff0\u7528\u4e8eNH3<\/sub>-SCO\u7684\u9ad8\u9009\u62e9\u6027CuOx<\/sub>\/PtCu\u50ac\u5316\u5242\u8868\u9762\u7684\u6676\u683c\u6c27\u8f85\u52a9i-SCR\u673a\u5236\uff09\u4e3a\u9898\u4e8e2023\u5e74\u53d1\u8868\u5728\u56fd\u9645\u8457\u540d\u671f\u520aACS Catalysis<\/em><\/strong><\/em><\/strong>\u4e0a\uff08https:\/\/pubs.acs.org\/doi\/10.1021\/acscatal.3c00314?ref=PDF\uff09\u3002\u534e\u4e2d\u79d1\u6280\u5927\u5b66\u6750\u6599\u5b66\u9662\u535a\u58eb\u5218\u8273\u98de\u4e3a\u7b2c\u4e00\u4f5c\u8005\uff0c\u6750\u6599\u5b66\u9662\u675c\u7eaf\u8001\u5e08\u548c\u5355\u658c\u6559\u6388\u4e3a\u8bba\u6587\u7684\u5171\u540c\u901a\u8baf\u4f5c\u8005\uff0c\u534e\u4e2d\u79d1\u6280\u5927\u5b66\u6750\u6599\u5b66\u9662\u535a\u58eb\u5218\u748b\u548c\u5f90\u6d01\u3001\u6e05\u534e\u5927\u5b66\u535a\u58eb\u738b\u6210\u96c4\u3001\u6606\u660e\u8d35\u91d1\u5c5e\u7814\u7a76\u6240\u8d75\u4e91\u6606\u6559\u6388\u3001\u5f20\u7231\u654f\u7814\u7a76\u5458\u3001\u534e\u4e2d\u79d1\u6280\u5927\u5b66\u673a\u68b0\u5b66\u9662\u5218\u6f47\u8001\u5e08\u3001\u6c5f\u897f\u79d1\u6280\u5e08\u8303\u5927\u5b66\u827e\u5efa\u5e73\u8001\u5e08\u53c2\u4e0e\u4e86\u5171\u540c\u53c2\u4e0e\u4e86\u8be5\u9879\u7814\u7a76\u5de5\u4f5c\u3002\u6b64\u9879\u5de5\u4f5c\u5bf9\u4e8e\u8bbe\u8ba1\u5f00\u53d1\u8fd1\u96f6\u6392\u653eASC\u50ac\u5316\u5242\u5177\u6709\u91cd\u8981\u610f\u4e49\u3002<\/p>\n\n\n

\n
\"\"<\/a>
\u56fe2\uff1a<\/strong>\u00a0(a) NH3<\/sub>\u6c27\u5316\u71c3\u70e7\u66f2\u7ebf\uff0c(b) Arrhenius\u56fe\uff0c(c) t\/Al2<\/sub>O3<\/sub>\u00a0IWI\u6837\u54c1(\u7eff\u8272)\uff0cPt-Al2<\/sub>O3<\/sub>\u00a0ST\u6837\u54c1(\u6a59\u8272)\u548cPtCu-Al2<\/sub>O3<\/sub>\u00a0ST\u6837\u54c1(\u7ea2\u8272)NH3<\/sub>- SCO\u7684N2<\/sub>\u9009\u62e9\u6027\u56fe\uff0c(d) PtCu-Al2<\/sub>O3<\/sub>\u00a0ST\u6837\u54c1\u5728190\u2103\u4e0b100\u5c0f\u65f6\u7684\u7a33\u5b9a\u6027\u6d4b\u8bd5\u3002(e)\u6c28\u548c\u6c27\u7684\u53cd\u5e94\u7ea7\u6570\u3002(f) PtCu-Al2<\/sub>O3<\/sub>\u00a0ST\u6574\u4f53\u50ac\u5316\u5242NH3<\/sub>-SCO\u6027\u80fd;(g)\u5c0f\u6837\u6d4b\u8bd5\u793a\u610f\u56fe\u3002<\/figcaption><\/figure><\/div>\n\n\n

\u5982\u56fe2<\/strong>\u6240\u793a\uff0cPtCu-Al2<\/sub>O3<\/sub>\u00a0ST\u5728141\u00a0\u00b0C\u65f6\u7684\u6c28\u8f6c\u5316\u7387\u4e3a50%\uff0c\u4f4e\u4e8ePt\/Al2<\/sub>O3<\/sub>\u00a0IWI\u7684213\u00a0\u00b0C\u548cPt-Al2<\/sub>O3<\/sub>\u00a0ST\u7684166\u00a0\u00b0C\uff0cN2<\/sub>\u9009\u62e9\u6027\u987a\u5e8f\u5982\u4e0b\uff1aPtCu-Al2<\/sub>O3<\/sub>\u00a0ST > Pt\/Al2<\/sub>O3<\/sub>\u00a0IWI > Pt-Al2<\/sub>O3<\/sub>\u00a0ST\u3002\u7279\u522b\u662f\uff0cPtCu-Al2<\/sub>O3<\/sub>\u00a0ST\u6837\u54c1\u5728170\u00b0C\u65f6\u5177\u670995%\u7684N2<\/sub>\u9009\u62e9\u6027\u548c90%\u7684\u6c28\u8f6c\u5316\u7387\uff0c\u8fd9\u662fAl2<\/sub>O3<\/sub>\u8d1f\u8f7d\u7684Pt\u57fa\u50ac\u5316\u5242\u4e2d\u6700\u9ad8\u7684N2<\/sub>\u9009\u62e9\u6027\uff0c\u800c\u4e14\u6ca1\u6709\u727a\u7272\u4f4e\u6e29NH3<\/sub>-SCO\u6d3b\u6027\u3002\u4e3a\u4e86\u8bc4\u4f30\u6240\u5f00\u53d1\u7684PtCu\u50ac\u5316\u5242\u5728H2<\/sub>O\u548cCO2<\/sub>\u539f\u6599\u6c14\u4e2d\u7684\u53ef\u9760\u6027\uff0c\u6211\u4eec\u8fdb\u4e00\u6b65\u6d4b\u8bd5\u4e86PtCu- Al2<\/sub>O3<\/sub>\u00a0ST\u5728\u5355\u7247\u6837\u54c1\u4e2d\u7684NH3<\/sub>-SCO\u6027\u80fd\uff0c\u5982\u56fe2f-g<\/strong>\u6240\u793a\u3002PtCu-Al2<\/sub>O3<\/sub>\u00a0ST\u6574\u4f53\u5f0f\u6837\u54c1\u7684T50<\/sub>\u548cT90<\/sub>\u5206\u522b\u4e3a184\u2103\u548c204\u2103\uff0c\u8fdc\u4f18\u4e8e\u5df2\u6709\u62a5\u9053\u7684\u53cc\u5c42\u5206\u5b50\u7b5b+Pt\/Al2<\/sub>O3<\/sub>\u5355\u7247\u50ac\u5316\u5242\u3002\u5e76\u5728H2<\/sub>O\u548cCO2<\/sub>\u53cd\u5e94\u6761\u4ef6\u4e0b\u8fdb\u884c\u4e86\u9009\u62e9\u6027\u8bd5\u9a8c\u3002\u6574\u4f53\u6837\u54c1\u5728250\u2103\u4ee5\u4e0b\u5177\u6709\u4e0e\u7c89\u672b\u50ac\u5316\u5242\u76f8\u5f53\u7684\u9009\u62e9\u6027\u3002\u5355\u5c42PtCu-Al2<\/sub>O3<\/sub>\u00a0ST\u6574\u4f53\u5f0f\u6837\u54c1\u7684\u9009\u62e9\u6027\u4ecd\u7136\u8fdc\u9ad8\u4e8e\u53cc\u5c42\u7ed3\u6784\u7684\u6574\u4f53\u5f0f\u50ac\u5316\u5242\uff0c\u8868\u660e\u5176\u9002\u7528\u6027\u3002<\/p>\n\n\n\n

\u50ac\u5316\u5242\u7684\u8d4b\u5b58\u72b6\u6001\u8868\u5f81\u5982\u56fe3<\/strong>\u6240\u793a\u3002\u50ac\u5316\u5242\u4e3b\u4f53\u4e3aAl2<\/sub>O3<\/sub>\u8d1f\u8f7d\u7684PtCu\u65e0\u5e8f\u5408\u91d1\u50ac\u5316\u5242\u3002\u7531\u4e8e\u5236\u5907\u8fc7\u7a0b\u4e2d\u51fa\u73b0\u4e86\u5408\u91d1\u7684\u504f\u6790\uff0c\u5408\u91d1\u8868\u9762\u51fa\u73b0\u4e86Cu\u7684\u5bcc\u96c6\uff0c\u5e76\u4e14\u88ab\u6c27\u5316\u4e3aCuOx<\/sub>\uff0c\u5f62\u6210\u4e86CuOx<\/sub>\/PtCu\u5fae\u754c\u9762\u3002<\/p>\n\n\n

\n
\"\"<\/a>
\u56fe3\uff1a<\/strong>(a)\u5404\u79cd\u50ac\u5316\u5242\u6837\u54c1\u7684XRD\u8c31\u56fe\uff0c(b) Cu 2p, Pt 4d XPS
\u8c31\uff0c(c) O 1s XPS\u8c31\uff1bPt\/Al2<\/sub>O3<\/sub>\u00a0IWI\u6837\u54c1(\u7eff\u8272)\uff0cPt-Al2<\/sub>O3<\/sub>\u00a0ST
\u6837\u54c1(\u6a59\u8272)\uff0cPtCu-Al2<\/sub>O3<\/sub>\u00a0ST\u6837\u54c1(\u7ea2\u8272)\u3002(d) HRTEM\u7ed3\u679c\uff0c
(e) HAADF-STEM\uff0c\u63d2\u56fe\u663e\u793aPtCu\u5408\u91d1\u5728PtCu-Al2<\/sub>O3<\/sub>\u00a0ST
\u6837\u54c1\u4e0a\u7684\u7ebf\u626b\u63cf\uff0cPtCu-Al2<\/sub>O3<\/sub>\u00a0ST\u6837\u54c1\u7684(f) Cu\u5143\u7d20\u548c(g) Pt
\u5143\u7d20\u7684mapping\u5206\u5e03\u56fe\u3002<\/figcaption><\/figure><\/div>\n\n\n

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